Air Vehicle Technology Integration Program (AVTIP). Delivery Order 0004: Advanced Sol-Gel Adhesion Processes

Abstract

This report summarizes optimization work for surface preparations and hybrid primers utilizing sol-gel technology on metal alloy substrates. The project focuses on the development and optimization of user-friendly sol-gel methods for preparing metal surfaces for bonding with 250 degrees F-cure and 350 degrees F-cure epoxy adhesives. Several improvements to the Boegel-EPII materials and processes were identified in this work. For example, addition of a surfactant can improve the appearance and uniformity of the sol-gel coatings, but is not critical for achieving good performance on these alloys. Studies indicate that careful choice of abrasive media and tools is required to achieve reproducible performance for the surface preparation of aluminum alloys. Under carefully controlled laboratory conditions, it is possible to yield good performance for many of the abrasive media, but when subjected to conditions that mimic a repair scenario, only a few of the abrasive media gave reproducible performance. Surface contamination on the metal was a result of smeared adhesive, overheating of the abrasive pad or tool, or unacceptable cleaning of the surface. Performance using downselected abrasive media and tools was verified using hot/wet testing, such as the wedge test and double cantilever beam testing. Procedures were documented specifying all of the preferred materials and processes.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Apr 01, 2002
Accession Number
ADA419183

Entities

People

  • Kay Y. Blohowiak
  • Kristina S. Preedy
  • Robert A. Anderson
  • Ronald R. Stephenson

Organizations

  • Phantom Works

Tags

Communities of Interest

  • Biomedical
  • Energy and Power Technologies
  • Human Systems
  • Space

DTIC Thesaurus Topics

  • Abrasives
  • Adhesion
  • Adhesives
  • Air Force Research Laboratories
  • Aircrafts
  • Alloys
  • Aluminum Alloys
  • Aluminum Oxides
  • Cantilever Beams
  • Chemistry
  • Failure Mode And Effect Analysis
  • Manufacturing
  • Materials
  • Metals
  • Performance Tests
  • Surface Chemistry
  • User Friendly

Fields of Study

  • Materials science

Readers

  • Software Engineering.
  • Surface Coatings Technology.
  • Systems Analysis and Design