Determination of Nickel, Nickel Chloride Hexahydrate and Boric Acid in Nickel Sulfamate Plating Solutions by Titration

Abstract

The chemical literature lacks analysis methods for the determination and adequate monitoring of nickel, nickel chloride hexahydrate and boric acid in nickel sulfamate plating solutions. Methods are given here that provide acceptable analysis and monitoring of these chemical species in this nickel sulfamate plating process. The optimum respective operating range of nickel, nickel chloride hexahydrate and boric acid are 53.0 -94.0 g/l, 6.0- 30.0 g/l, and 30.0-45.0 g/l. The resulting precisions are in the range of 0- 0.3 g/l providing adequate monitoring of these plating solutions supported by two years of testing. chemical analysis, nickel, nickel chloride hexahydrate, boric acid, nickel sulfamate plating solutions, titration

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1991
Accession Number
ADA420005

Entities

People

  • Samuel Sopok

Organizations

  • United States Army Armament Research, Development and Engineering Center

Tags

DTIC Thesaurus Topics

  • Acids
  • Analytical Chemistry
  • Analytical Chemistry Techniques
  • Boric Acids
  • Buffers (Chemistry)
  • Chemical Analysis
  • Chemical Synthesis
  • Chemistry
  • Engineering
  • Hydroxides
  • Materials
  • Silver Compounds
  • Sodium Hydroxide
  • Standards
  • Test Methods
  • Titration

Fields of Study

  • Chemistry

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Manufacturing Engineering.
  • Metallurgy