In Vitro Rat Hepatocyte Toxicity and Bacteria Genotoxicity Evaluation of High Energy Chemicals for Replacement of Hydrazine

Abstract

In an effort to develop methods to predict the toxicological response of newly synthesized chemicals that are of interest to the US Air Force, in vitro rat hepatocyte toxicity and bacteria (Salmonella) genotoxicity assays were performed on thirteen high-energy chemicals (HEC) that were selected as potential replacements of hydrazine. The HECs were primarily hydrazine derivatives (hydrazinium nitrate, HZN; 2-hydroxyethylhydrazine nitrate, HEHN; diethyl hydrazine nitrate, DEHN; 1,4- nitrate, DHTN; methylhydrazine nitrate, MHN; diaminogaanidine nitrate, DAGN; 2,2-dimethyltriazanium nitrate, DMTN; nitroaminogaanidine nitrate, NAGN), amino containing compounds (ethanolamine nitrate, EAN; histamine dinitrate, HDN; methoxylamine nitrate, MAN), and triazole containing compounds (1,2,-triazole nitrate, TN; 4-amino-l,2,4-triazole nitrate, ATN). The results in hepatocytes showed a dose dependent decrease in mitochondrial activity (MTT), increase in lactate dehydrogenase (LDH) leakage, and depletion of GSH levels. Responses to hydrazine were used as reference values for ranking the other HECs. According to the MTT assay, the hydrazine-containing compounds are the most toxic (HZN> DEHN> DHTN > MHN > HEHN > DAGN > NAGN), amino-containing compounds displayed medium toxicity (HDN > EAN > MAN) and triazole-containing compounds exhibited low toxicity (DMTN > ATN > TN). Results of genotoxicity (Ames assay) on 10 of the 13 HECs indicated that HZN, DHTN and MAN were mutagenic. DHTN was a direct mutagen causing AT and GC base-pair substitutions and frameshift mutations.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 2002
Accession Number
ADA424199

Entities

People

  • D. Mattle
  • J. Frazier
  • P. Qao
  • S. Husain
  • Sanchit Sharma

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Air Force
  • Air Force Research Laboratories
  • Amines
  • Bacteria
  • Biological Sciences
  • Cells
  • Chemistry
  • Culture Media
  • Drug Abuse
  • Epithelial Cells
  • Free Radicals
  • High Energy
  • Hydrazine Derivatives
  • Hydrazines
  • Mutagenicity Tests
  • Sodium Compounds
  • Toxicity

Fields of Study

  • Chemistry

Readers

  • Data Mining and Knowledge Discovery.
  • Organic Chemistry
  • Toxicology/Environmental Toxicology