Taming Hazardous Reactive Materials for Single Crystal X-ray Diffraction Studies: Dealing with Handling and Disorder Nightmares

Abstract

Partial Contents; The challenging transition I, The exciting world of high nitrogen chemistry, why Carbon forms polymers and Nitrogen does not?, N-F Compounds, What is So Unusal About the N5+ Cation?, Selection of Suitable Starting Materials for N5+ Synthesis, Fluorodiazonium Salts; Crucial Intermediates in Polynitrogen Chemistry, Right Tools for the Right Job, Fluorodiazonium Salts: Crucial Intermediates in Polynitrogen Chemistry, Right Tools for the Right Job, Reactions of trans-N2F2 with SbF5?, Using "inert" organic solvents, Recrystallization, Mounting using LT apparatus, Hungry for cryoloops?, Ball and Stick Representation of NF4Sb2F11, Molecular Structure of N2F SbF6, Crystal Packing Diagram of N2F SbF6(c-axis).

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Document Details

Document Type
Technical Report
Publication Date
May 26, 2004
Accession Number
ADA425523

Entities

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Energy and Power Technologies
  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Air Force
  • Air Force Research Laboratories
  • Chemistry
  • Crystal Structure
  • Crystals
  • Diffraction
  • Diseases And Disorders
  • Energy
  • Low Temperature
  • Materials
  • Military Research
  • Reactive Materials
  • Single Crystals
  • Thermodynamics
  • Valence Bond Theory
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Chemistry

Readers

  • Educational Psychology
  • Materials Science and Engineering.
  • Organic Chemistry