Nanostructured High-Performance Materials Consisting of Bismaleimide and Functional Liquid Crystal Monomer

Abstract

We have synthesized a liquid-crystalline monomer, 12-4-CYANOBIPHENYL-4-OXY dodecanoic acid (11CN-COOH), and then grafted it onto the DABPA and then cured the 11CN-COOH-grafted DABPA with BMPM, yielding BMI resin functionalized with liquid crystal monomer. In so doing, we have elucidated the reaction (cure) mechanism between 11CN-COOH-grafted DABPA and BMPM using Fourier transform infrared (FTIR) spectroscopy. Thermal transition temperatures before and after the cure of BMI resin and also functionalized BMI resin were measured using differential scanning calorimetry. Micrographs of BMI resin and also functionalized BMI resin were obtained using optical microscopy. Finally, the mechanical properties of cured BMI and functionalized BMI resins were measured. It has been found that the flexural modulus of functionalized BMI resin is about two times greater than that of neat BMI resin, indicating that the addition of liquid crystalline monomer has enhanced the toughness of BMI resin.

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Document Details

Document Type
Technical Report
Publication Date
Nov 01, 2004
Accession Number
ADA428496

Entities

People

  • Chang D. Han

Organizations

  • University of Akron

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Calorimetry
  • Chemical Reactions
  • Chemistry
  • Crystals
  • Electron Microscopes
  • Electron Microscopy
  • Imides
  • Impact Strength
  • Liquid Crystals
  • Materials
  • Mechanical Properties
  • Microscopy
  • Scanning
  • Spectroscopy
  • Toughness
  • Transition Temperature
  • Transitions

Fields of Study

  • Materials science

Readers

  • Microbial Pathology
  • Polymer Science and Technology
  • Solar Photovoltaics and Thermoelectric Devices.

Technology Areas

  • Microelectronics