Multidisciplinary Oxygen Atom Erosion and Surface Characterization Studies of Polyhedral Oligomeric Silsesquioxane

Abstract

The objectives of this research project have been to characterize the degradation of various types of polymers under simulated space (low-earth orbit (LEO)) conditions and to develop polymers for spacecraft coatings which have improved survivability in LEO. Many polymers have been tested including kapton, polyethylene, fluoromers, polyhedral oligomeric silsequioxane (POSS)-containing copolymers and others. The testing was performed in an ultrahigh vacuum system which contained an atomic oxygen (AO) source and a vacuum ultraviolet (vuv) source. In some studies the polymers were also exposed to energetic electrons and ions. The chemical alterations occurring during the degradation was monitored using X-ray photoelectron spectroscopy (XPS). All polymers exhibit large chemical changes. The POSS-containing polymers are particularly interesting for space applications because they form a thin silica layer which protects the underlying polymer from further degradation.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Dec 14, 2004
Accession Number
ADA429964

Entities

People

  • Gar Holfund

Organizations

  • University of Florida

Tags

Communities of Interest

  • Space

DTIC Thesaurus Topics

  • Chemical Engineering
  • Chemisorption
  • Chemistry
  • Earth Orbits
  • Electrons
  • Films
  • Fluoropolymers
  • High Resolution
  • Kinetic Energy
  • Low Earth Orbits
  • Photoelectrons
  • Polymers
  • Radiation
  • Spectroscopy
  • Ultraviolet Radiation
  • X Ray Photoelectron Spectroscopy
  • X Rays

Fields of Study

  • Materials science

Readers

  • Plasma Physics.
  • Polymer Science and Technology
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene
  • Space