NMR Method for the Quantitative Analysis of VX Hydrolysates

Abstract

This procedure is based on previously published ERDEC-TR-449, Nuclear Magnetic Resonance (NMR) Analysis of Chemical Agents and Reaction Masses Produced by their Chemical Neutralization and unpublished work entitled NMR Method for the Quantitative Purity Analysis of Feedstock Samples. This procedure uses an internal standard to establish an absolute weight percent for the analytes in question. Identifying the structures of other components in the mixture is not necessary. The weight percent calculations are not negatively affected by the presence of undetectable components (e.g., elemental sulfur, inorganic salts, etc.) in the sample.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 2005
Accession Number
ADA430360

Entities

People

  • David J. Mcgarvey
  • H. D. Durst
  • Mark D. Brickhouse
  • Richard J. O'connor
  • William R. Creasy

Tags

Communities of Interest

  • Advanced Electronics
  • Counter WMD

DTIC Thesaurus Topics

  • Chemical Shifts
  • Chemical Warfare Agents
  • Chemistry
  • Corporations
  • Data Analysis
  • Detection
  • Engineering
  • Frequency
  • Magnetic Resonance
  • Materials
  • Molecular Weight
  • Nuclear Magnetic Resonance
  • Operating Systems
  • Organic Compounds
  • Resonance
  • Spectra
  • Standards

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  • Analytical Chemistry