Tensile Stress Rupture Behavior of a Woven Ceramic Matrix Composite in Humid Environments at Intermediate Temperature

Abstract

Stress rupture tests on the Sylramic(TM) fiber with an in-situ layer of boron nitride, boron nitride interphase, and SiC matrix ceramic matrix composite were performed at 550 degrees C and 750 degrees C with 0.0, 0.2, or 0.6 atm partial pressure of water vapor, pH(sub 2)O. The 550 degrees C, 100-hr strengths were 75%, 65% and 51% of the monotonic room temperature tensile strength, respectively. At 750 degrees C, the strengths were 67%, 51%, and 49%, respectively. Field Emission Scanning Electron Microscopy analysis estimated the total embrittlement times for 550 degrees C with 0.0, 0.2, and 0.6 atm pH(sub 2)O were >63 hrs, >38 hrs, and between 8 and 71 hrs, respectively. Corresponding estimated embrittlement times for the 750 degrees C were >83 hrs, between 13 and 71 hrs, and between 1 and 6 hrs. A time-dependent, phenomenological, Monte Carlo-type failure model was developed and simulated total embrittlement times that were within the experimentally determined range for all cases. Variation in the room temperature ultimate strength, the elevated temperature ultimate strength, and the fiber reference strength affected the model the most. Variation in the modulus of elasticity of the matrix and fiber affected it the least. Stress rupture strength degradation increases with temperature, moisture content level, and exposure time.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Mar 01, 2005
Accession Number
ADA431532

Entities

People

  • Kevin J. Larochelle

Organizations

  • Air Force Institute of Technology

Tags

Communities of Interest

  • Air Platforms
  • Energy and Power Technologies
  • Weapons Technologies

DTIC Thesaurus Topics

  • Arrhenius Equation
  • Ceramic Materials
  • Ceramic Matrix Composites
  • Chemical Reactions
  • Chemistry
  • Composite Materials
  • Creep
  • Elastic Properties
  • Electron Microscopy
  • Material Degradation Processes
  • Materials
  • Mechanical Properties
  • Mechanics
  • Modulus Of Elasticity
  • Stress Strain Relations
  • Stresses
  • Tensile Strength

Readers

  • Materials Science (Mechanical Engineering).
  • Mathematics or Statistics
  • Reinforced Composite Materials

Technology Areas

  • Microelectronics