Microwave Induced Reaction of H-Dimethylphosphonate With Styrene Oxide
Abstract
The reaction of a neat mixture of styrene oxide and H-dimethyl-phosphonate under microwave catalysis and without any solvent for six minutes furnished a complex mixture containing dimethyl methylphosphonate, trimethylphosphate, phenylacetaldehyde, 1-methoxy-2- phenylethanol, 1-phenylethleneglycol, cis- and trans-1, 3-diphenylcyclobutanes, hydrogen 1-(2- phenylethyl)methylphosphinate, (1-phenylethyl)dimethylphosphonate and (1-phenylethyl)- dimethylphosphonate via free radical processes. The mechanism of formation of the said compounds and their GC-MS characterization are described herein.
Document Details
- Document Type
- Technical Report
- Publication Date
- Jan 01, 2002
- Accession Number
- ADA436045
Entities
People
- D. K. Rohrbaugh
- F. R. Longo
- G. W. Wagner
- H. Dupont Durst
- S. Munavalli
Organizations
- Edgewood Chemical Biological Center