Improving the D2512 Lox Compatibility of Composites by Using Thermally Conductive Graphite Fibers

Abstract

This effort demonstrated that using a thermally conductive fiber substantially enhances a composite's ASTM D2512 mechanical impact liquid oxygen compatibility. It repeatedly achieved 90% of the goal of passing D2512 with a 1700% improvement over baseline. This effort also documented the types of fracture surfaces routinely found in the residuals of the materials investigated. These fracture surfaces indicate that hertzian fracture is the mechanism by which a specimen fractured and failed. The fracture surfaces routinely indicated that kinetic friction associated with signs of intense heating occurred. Kinetic friction's mechanical-to-thermal transformation mechanism provided the only phenomenological explanation for the extremely rapid and large temperature rises required for conditions recognizable as ignition to occur in the time frame of a D2512 test. The effort crystallized the sequence from fracture to heating to ignition. First, a series of hertzian fractures develop. These allow kinetic friction of the hertzian fractured material to occur. Kinetic friction transforms mechanical energy into temperature rising thermal energy. This thermal energy causes the material to degrade by radical chain scission and oxidize by radical addition peroside chemistry to a degree detectable as ignition.

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Document Details

Document Type
Technical Report
Publication Date
Sep 01, 2005
Accession Number
ADA443342

Entities

People

  • Roger Gerzeski

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Air Platforms
  • Biomedical
  • Energy and Power Technologies
  • Weapons Technologies

DTIC Thesaurus Topics

  • Biomedical And Dental Materials
  • Chemical Synthesis
  • Chemistry
  • Material Degradation Processes
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Plastics
  • Polymer Chemistry
  • Polymer Degradation
  • Polymeric Films
  • Reinforced Plastics

Readers

  • Rocket Propulsion.
  • Structural Health Monitoring of Composite Structures.
  • Thin Film Deposition Science.