A study of Sensitization in Types 301 and 304L Stainless Steels Using Mossbauer Spectroscopy

Abstract

A relatively new research tool has been brought to bear on a relatively old problem. Mossbauer effect spectroscopy in conjunction with x-ray diffraction techniques were used to study the phenomenon of stainless steel sensitization. A ferromagnetic phase, thought to be pseudomartensite, has been found to exist in sensitized Type 301. Stresses generated in the matrix by morphology changes of the precipitated carbides is deemed responsible for the creation of this phase. No such phase was detected in the Type 304L. It was confirmed that the precipitated carbides were of the complex type (Cr,Fe)23C6. Furthermore, it was established that these carbides are paramagnetic. In the presence of austenite, the Mossbauer peak for the carbides is overshadowed. In single phase materials grain size has no effect on the Mossbauer spectrum. In multi-phase materials the peak locations are unaffected by grain size, but quantitative evaluations are influenced.

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 1968
Accession Number
ADA453761

Entities

People

  • O. W. Albritton

Organizations

  • Louisiana State University

Tags

DTIC Thesaurus Topics

  • Austenite
  • Chemical Synthesis
  • Chemistry
  • Chromium
  • Cold Working
  • Diffraction
  • Grain Size
  • Iron
  • Iron Alloys
  • Martensite
  • Materials
  • Spectra
  • Spectroscopy
  • Stainless Steel
  • Steel
  • X Rays
  • X-Ray Diffraction

Fields of Study

  • Physics

Readers

  • Powder metallurgy of Titanium alloys.
  • Quantum spin resonance or Electron Paramagnetic Resonance spectroscopy.
  • Systems Analysis and Design