Composites Containing Barrier Layers for Reduced Permeability at Cryogenic Temperatures

Abstract

To help prevent leakage that may occur if cracks develop in a cryogenic composite pressure vessel due to thermo-mechanical fatigue, liners are occasionally implemented. However, liners can be difficult to fabricate and maintain, and mismatch of their CTE with the underlying composite can promote debonding of the liner. In this effort, two approaches to incorporating a barrier layer directly into a carbon/bismaleimide PMC (IM7/5250-4) were investigated for their effectiveness in preventing the development of through-thickness crack networks that can lead to leakage. In the first concept, a "thin ply" of T800 carbon fiber/5250-4 bismaleimide composite much thinner than a standard 0.13 mm thick ply was placed adjacent to the surface plies or mid-plane ply group where cracks initiated first. This arrangement was chosen to help prevent crack growth beyond these early-cracking plies. Overall the thin plies were successful both in limiting "stitch crack" propagation into the neighboring plies and in limiting the overall interior ply damage. In the second concept, an even thinner layer (<0.25 mm thick) of electro-spun PAN fibers infused with 5250-4 was again placed next to the surface plies. The electro-spun fiber layer did not prevent crack growth from the surface plies into the neighboring plies but did significantly limit the interior ply damage that formed.

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Document Details

Document Type
Technical Report
Publication Date
Mar 01, 2006
Accession Number
ADA461295

Entities

People

  • Ran Y. Kim
  • Steven L. Donaldson
  • Vernon T. Bechel

Organizations

  • University of Dayton

Tags

Communities of Interest

  • Air Platforms
  • Energy and Power Technologies
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force
  • Air Force Research Laboratories
  • Carbon Fibers
  • Composite Materials
  • Delamination
  • Epoxy Composites
  • Epoxy Laminates
  • Fibers
  • Laminates
  • Materials
  • Materials Processing
  • Military Research
  • Permeability
  • Polymer Matrix Composites
  • Pressure Vessels
  • Standards
  • Thickness

Fields of Study

  • Materials science

Readers

  • Reinforced Composite Materials
  • Structural Health Monitoring of Composite Structures.