Measured Leak Rate of Ammonia Through an Epoxy/Stainless-Steel Patch

Abstract

A program has experienced pitting corrosion in anhydrous ammonia-charged loop heat pipes. Areas of each loop heat pipe with increased risk of pitting corrosion were previously identified with X-ray image analysis and patched with a formed stainless-steel cap, bonded with a space-approved epoxy. To assess the lifetime of the patch and sensitivity to manufacturing variation, simulated leaks in circular aluminum discs were patched with several different variants on the same epoxy-stainless materials system. The patches were aged at elevated temperature to accelerate degradation phenomena. No gross failures of the patches were observed in four weeks of testing. No significant difference was observed between the aged bonded material at 353K, 393K, or a freshly prepared patch. Infrared detection of ammonia leaking through the patch suggests that a loss rate of 0.16 +/- 0.04 mg of ammonia per year will occur through the simulated leaks with primed patches.

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Document Details

Document Type
Technical Report
Publication Date
Aug 10, 2007
Accession Number
ADA474731

Entities

People

  • B. B. Brady
  • J. D. Desain
  • T. J. Curtiss

Organizations

  • The Aerospace Corporation

Tags

Communities of Interest

  • Advanced Electronics
  • Sensors
  • Space

DTIC Thesaurus Topics

  • Aluminum
  • Aluminum Foil
  • Chemical Reactions
  • Chemistry
  • Corrosion
  • Detection
  • Detectors
  • Heat Pipes
  • Infrared Detection
  • Materials
  • Materials Laboratories
  • Microelectromechanical Systems
  • Radiation
  • Space Systems
  • Spectra
  • Stainless Steel
  • X Rays

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Space/Atmospheric Physics.
  • Surface Coatings Technology.

Technology Areas

  • Space
  • Space - Hall-Effect Thruster