Laboratory Determination of Thermal Protection System Materials Surface Catalytic Properties

Abstract

Different experimental approaches to measuring catalytic reaction efficiencies on thermal protection system materials are reviewed. Special emphasis is given to the theory and application of the diffusion tube side-arm reactor technique. In this technique, reactants diffuse into a dead-end tube and are progressively removed from the gas phase by surface reactions on the walls, establishing unique steady-state concentration profiles along the length of the tube. Reactant loss probabilities are determined by matching experimentally measured species profiles to calculated solutions of a reaction-diffusion model. The advantages of laser-based methods for species concentration measurements are summarized and different approaches to reactor modeling and the extraction of reaction efficiencies from measured data are presented. The advantages and limitations of the diffusion-tube side-arm technique, the associated uncertainties in derived loss probabilities, and the prospects for further laboratory development, are presented.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 2007
Accession Number
ADA476528

Entities

People

  • Jochen Marschall

Organizations

  • SRI International

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Reactions
  • Chemistry
  • Computational Fluid Dynamics
  • Energy
  • Energy Transfer
  • Laser Beams
  • Laser Dyes
  • Laser Induced Fluorescence
  • Materials
  • Measurement
  • Physics Laboratories
  • Recombination Reactions
  • Simulations
  • Steady State
  • Surface Chemistry
  • Surface Reactions
  • Two Dimensional

Fields of Study

  • Chemistry
  • Environmental science

Readers

  • Combustion and Flow Dynamics.
  • Mathematical Modeling and Probability Theory.
  • Nanocomposite Materials Science

Technology Areas

  • Directed Energy