Determination of Volatile Organic Compounds Content Using Novel Ash and Total Solids Analysis for Chemical Agent Resistant Coating Systems

Abstract

Volatile organic compounds (VOCs) found in coatings are a major concern of the U.S. Army Research Laboratory, the Environmental Protection Agency (EPA), and local air quality boards. The current laboratory standards used to determine VOCs in Chemical Agent Resistant Coating and other military coating systems are EPA Method 24 or American Society for Testing and Materials ASTM D 3960. It has been reported that VOC measurements using this method produce errors that increase nearly exponentially at VOC concentrations <2.1 lb/gal (250 g/L). The solids or nonvolatile component of the coating takes 1.5 hr to measure by oven, and the ash takes multiple hours as described in ASTM D 3723. These values are necessary to validate VOCs; the primary goal is to minimize VOCs in all coatings. This report outlines experimentation to quantify actual VOC levels of formulated paints using both EPA Method 24 and a proposed alternative test method that utilizes a moisture analyzer. Analysis of the results verified comparable accuracy between the current process and the instrumental-based method, with the latter process producing a more rapid result.

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Document Details

Document Type
Technical Report
Publication Date
Oct 01, 2008
Accession Number
ADA494061

Entities

People

  • Daniel Pope
  • Pauline Smith
  • William Lum

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Accuracy
  • Analyzers
  • Chemical Warfare Agents
  • Errors
  • Materials
  • Measurement
  • Military Research
  • Moisture
  • Organic Compounds
  • Standards
  • Test Methods
  • Volatile Organic Compounds
  • Waterborne

Readers

  • Computational Modeling and Simulation
  • Environmental Engineering.
  • Surface Coatings Technology.