Probing and Manipulating Protein Conformation Changes by Time-Resolved Single-Molecule Spectroscopy and Site-Specific Ultramicroscopy

Abstract

This project was to develop and demonstrate a novel single-molecule spectroscopy and imaging technique to support the DARPA program on Control of Protein Conformations. The goal of our project is to advance, integrate, and apply cutting-edge atomic force microscopy (AFM) and single-molecule imaging techniques to control and analyze the protein conformational changes and according activity changes through AFM force manipulation and fluorescence resonant energy transfer (FRET) measurements as a function of local site geometry and molecular structure. In this project, we have focused our demonstration and study on controlling protein conformations to manipulate the enzyme reactivity, affinity, and selectivity. Our approach has been to use AFM tip to control protein conformational states and to apply single-molecule FRET imaging to measure the protein enzyme activity in real time. Our progress towards the demonstration of the new technology has provided an unprecedented advancement on a high spatially (nanometers) and temporally (micro's to seconds) resolved single-molecule spectroscopy of optically and mechanically controlling single-molecule protein conformational changes and activities.

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 2008
Accession Number
ADA500765

Entities

People

  • H. P. Lu

Organizations

  • Bowling Green State University

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Abstracts
  • Amino Acids
  • Bacterial Proteins
  • Buffers (Chemistry)
  • Chemistry
  • Confocal Microscopy
  • Correlation Analysis
  • Detection
  • Detectors
  • Energy Transfer
  • Imaging Techniques
  • Materials
  • Microscopes
  • Microscopy
  • Molecules
  • Physical Theories
  • Spectroscopy

Fields of Study

  • Physics

Readers

  • Distributed Systems and Data Platform Development
  • Molecular and Cellular Biochemistry
  • Nanoscale Plasmonic Nanotechnology