Chemical Degradation of PCBs in Alaskan Soils

Abstract

Previous work suggested that the addition of lime could promote the removal of polychlorinated biphenyls (PCBs), presumably by alkaline hydrolysis reactions. A study was conducted to determine if a modified process (substituting sodium hydroxide (NaOH) for lime) could be used to treat PCB-contaminated soils in remote areas of Alaska. Experiments in which soils were reacted with 2% NaOH and a NaOH/zero valent iron mixture resulted in an approximate 20 to 30% reduction of Aroclor concentration compared to the controls. Tests applying Tween 80 at 15% (w/w) with NaOH at 2% (w/w) indicated that the Tween 80 increased PCB release from soil, but no significant PCB degradation was found. An experiment was then conducted to investigate the use of persulfate to treat PCBs in solution. Heat-activated (50 C) sodium persulfate (Na2S2O8) removed >90% of the PCBs (Aroclor 1254), but lime-activated persulfate was ineffective. A final study was conducted to investigate the effect of hydroxide and lime on PCB extraction and the effect of pH neutralization. The study was inconclusive, as it did not appear any net losses were demonstrated. The overall study indicated that alkaline hydrolysis does not appear to be effective for the treatment of the subject Alaska soils. Some promise might be found for heat-activated persulfate treatment, although the more easily applied lime activation was not effective.

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Document Details

Document Type
Technical Report
Publication Date
Apr 01, 2011
Accession Number
ADA541875

Entities

People

  • Agnes B. Morrow
  • Catherine C. Nestler
  • Charles Coyle
  • Scott Waisner
  • Victor Frank Medina

Organizations

  • Engineer Research and Development Center

Tags

Communities of Interest

  • Biomedical

DTIC Thesaurus Topics

  • Aqueous Solutions
  • Biphenyl
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Chlorides
  • Decomposition
  • Engineering
  • Health Services
  • Hydrolysis
  • Hydroxides
  • Neutralization
  • Organic Chemistry
  • Organic Compounds
  • Polychlorinated Biphenyls
  • Sodium Hydroxide
  • Water

Readers

  • Aquatic Ecology
  • Groundwater Contamination Remediation.
  • Mathematics or Statistics