Thermal Decomposition of 1,5-Dinitrobiuret (DNB): Direct Dynamics Trajectory Simulations and Statistical Modeling

Abstract

A large set of quasi-classical, direct dynamics trajectory simulations were performed for decomposition of 1, 5-dinitrobiuret (DNB) over a temperature range from 4000 to 6000 K, aimed at providing insight into DNB decomposition mechanisms. The trajectories revealed various decomposition paths, and reproduced the products (including HNCO, N2O, NO2, NO, and water) observed in DNB pyrolysis experiments. Using trajectory results as a guide, structures of intermediate complexes and transition states that might be important for decomposition were determined using density function theory calculations. Rice-Ramsperger-Kassel-Marcus (RRKM) theory was then utilized to examine behaviors of the energized reactant and intermediates and to determine unimolecular rates for crossing the various transition states. According to RRKM predictions, the dominant initial decomposition path of energized DNB corresponds to elimination of HNNO2H via a concerted mechanism where the molecular decomposition is accompanied with intra-molecular H-atom transfer from the central nitrogen to the terminal nitro oxygen. Other important paths correspond to elimination of NO2 and H2NNO(pi). NO(2) elimination is a simple N-N bond scission process. Formation and elimination of nitramide is however dynamically complicated, requiring twisting a -NHNO2 group out of the molecular plane, followed by an intramolecular reaction to form nitramide before its elimination. These two paths become significant at temperature above 1500 K, accounting for greater than 17% of DNB decomposition at 2000 K. This work demonstrates that quasi-classical trajectory simulations, in conjunction with electronic structure and RRKM calculations, are able to extract mechanisms, kinetics, dynamics and product branching ratios for the decomposition of complex energetic molecules, and predict how they vary with decomposition temperature.

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Document Details

Document Type
Technical Report
Publication Date
May 03, 2011
Accession Number
ADA547366

Entities

People

  • Ghanshyam L Vaghjiani
  • Jianbo Liu
  • Steven D Chambreau

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force Research Laboratories
  • Chemical Kinetics
  • Chemical Reaction Properties
  • Chemistry
  • Decomposition
  • Dynamics
  • Endothermic Reactions
  • Energetic Materials
  • Exothermic Reactions
  • First Principles Calculations
  • Heat Of Formation
  • Kinetics
  • Physical Chemistry
  • Potential Energy
  • Pyrolysis
  • Quantum Chemistry
  • Spectroscopy

Readers

  • Computational Modeling and Simulation
  • Organic Chemistry
  • Quantum Chemistry

Technology Areas

  • Microelectronics