Dislocation Decorrelation and Relationship to Deformation Microtwins during Creep of a Gamma' Precipitate Strengthened Ni-based Superalloy

Abstract

The evolution of microtwins during high temperature creep deformation in a gamma' strengthened Ni-based superalloy has been investigated through a combination of creep testing, transmission electron microscopy (TEM), theoretical modeling, and computer simulation. Experimentally, microtwin nucleation sources were identified and their evolution was tracked by characterizing the deformation substructure at different stages of creep deformation. Deformation is highly localized around stress concentrators such as carbides, borides and serrated grain boundaries, which act as sources of a/2(110) matrix-type dislocations. Due to fine channels between the gamma' particles coupled with a low gamma matrix stacking fault energy, the a/2(110) matrix dislocations dissociate into a/6(112) Shockley partials, which were commonly observed to be decorrelated from one another, creating extended intrinsic stacking faults in the c matrix. Microtwins are common and form via Shockley partial dislocations, cooperatively shearing both the gamma and gamma' phases on adjacent {1 1 1} glide planes. The TEM observations lead directly to an analysis of dislocation-precipitate interactions. The important processes of dislocation dissociation and decorrelation were modeled in detail through phase field simulations and theoretical analyses based on Orowan looping, providing a comprehensive insight into the microstructural features and applied stress conditions that favor the microtwinning deformation mode in gamma' strengthened Ni-based superalloys.

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Document Details

Document Type
Technical Report
Publication Date
Nov 01, 2011
Accession Number
ADA550602

Entities

People

  • Chao Shen
  • L. Kovarik
  • M. J. Mills
  • Nan Zhou
  • R. R. Unocic
  • Yaonan Wang

Organizations

  • Oak Ridge National Laboratory

Tags

Communities of Interest

  • Air Platforms

DTIC Thesaurus Topics

  • Boundaries
  • Chemical Compounds
  • Chemistry
  • Crystal Structure
  • Crystals
  • Electron Microscopy
  • Grain Boundaries
  • High Temperature
  • Materials
  • Materials Engineering
  • Materials Science
  • Mechanical Properties
  • Particles
  • Shear Stresses
  • Simulations
  • Transmission Electron Microscopy
  • Turbines

Fields of Study

  • Materials science

Readers

  • Materials Science and Engineering.
  • Powder metallurgy of Titanium alloys.

Technology Areas

  • Microelectronics