Effects of Silicon Substitution in the Main Chain Network Segments of Polycyanurates

Abstract

The incorporation of silicon into thermosetting polymers at the molecular level has been shown to have several significant effects, beyond improving thermo-oxidative stability, as demonstrated by studies of silicon-containing cyanate ester resins. These effects are generally traceable to the enhanced flexibility afforded by the substitution of C-Si and C-C bonds, and include increased free volume and thermal expansion. In cyanate esters, the increased specific volume leads to a decrease in cyanate ring density, which may explain the reduced water uptake in silicon-containing cyanate esters at high conversions. In addition, the increased flexibility provides for a greater degree of cure at lower temperatures than would otherwise be possible, leading, counterintuitively, to a higher glass transition temperature for a given cure schedule. Due to the molecular level mechanisms involved, many of these effects are expected to be present in other silicon-containing thermosetting resins as well.

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Document Details

Document Type
Technical Report
Publication Date
Nov 29, 2011
Accession Number
ADA555878

Entities

People

  • Andrew J. Guenthner
  • Joseph M Mabry
  • Josiah T. Reams
  • Kevin R. Lamison
  • Vandana Vij

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Abstracts
  • Air Force
  • Air Force Research Laboratories
  • Department Of Defense
  • Glass Transition Temperature
  • Information Operations
  • Military Research
  • Resilience
  • Resins
  • Specific Volume
  • Thermal Expansion
  • Thermosetting Plastics
  • Transition Temperature

Fields of Study

  • Materials science

Readers

  • Polymer Science and Engineering.