Atomic-Scale Investigation of Graphene Grown on Cu Foil and the Effects of Thermal Annealing

Abstract

We have investigated the effects of thermal annealing on ex-situ chemically vapor deposited submonolayer graphene islands on polycrystalline Cu foil at the atomic-scale using ultrahigh vacuum scanning tunneling microscopy. Low-temperature annealed graphene islands on Cu foil (at ~430 deg C) exhibit predominantly striped Moire patterns, indicating a relatively weak interaction between graphene and the underlying polycrystalline Cu foil. Rapid high-temperature annealing of the sample (at 700 800 C) gives rise to the removal of Cu oxide and the recovery of crystallographic features of the copper that surrounds the intact graphene. These experimental observations of continuous crystalline features between the underlying copper (beneath the graphene islands) and the surrounding exposed copper areas revealed by high-temperature annealing demonstrates the impenetrable nature of graphene and its potential application as a protective layer against corrosion.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 2011
Accession Number
ADA559902

Entities

People

  • Brandon Fisher
  • Esmeralda N. Yitamben
  • Helin Cao
  • Jeffrey R Guest
  • Jifa Tian
  • Jongweon Cho
  • Li Gao
  • Qingkai Yu
  • Wei Wu
  • Yong P. Chen

Organizations

  • Purdue University

Tags

DTIC Thesaurus Topics

  • Advanced Materials
  • Annealing
  • Chemical Vapor Deposition
  • Crystal Structure
  • Crystals
  • Films
  • Graphene
  • Heat Treatment
  • High Temperature
  • Low Temperature
  • Material Degradation Processes
  • Materials
  • Materials Processing
  • Materials Science
  • Measurement
  • United States
  • Vapor Deposition

Fields of Study

  • Physics

Readers

  • Materials Science and Engineering.
  • Nanoscale Plasmonic Nanotechnology
  • Quantum Dot Semiconductor Device Photonics and Graphene Optoelectronic Materials and THz Physics.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene