Surface Characterization and Direct Bioelectrocatalysis of Multicopper Oxidases (POSTPRINT)

Abstract

Multicopper oxidases (MCO) have been extensively studied as oxygen reduction catalysts for cathodic reactions in biofuel cells. Theoretically, direct electron transfer between an enzyme and electrode offers optimal energy conversion efficiency providing that the enzyme/electrode interface can be engineered to establish efficient electrical communication. In this study, the direct bioelectrocatalysis of three MCO (Laccase from Trametes versicolor, bilirubin oxidase (BOD) from the fungi Myrothecium verrucaria and ascorbate oxidase (AOx) from Cucurbita sp.)wasinvestigated and compared as oxygen reduction catalysts. Protein film voltammetry and electrochemical characterization of the MCO electrodes showed that DET had been successfully established in all cases. Atomic force microscopy imaging and force measurements indicated that enzyme was immobilized as a monolayer on the electrode surface. Evidence for three clearly separated anodic and cathodic redox events related to the Type 1 (T1) and the trinculear copper centers (T2, T3) of variousMCOwasobserved. The redox potential of the T1 centerwasstrongly modulated by physiological factors including pH, anaerobic and aerobic conditions and the presence of inhibitors.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 2010
Accession Number
ADA562418

Entities

People

  • Constantine Khripin
  • Dmitri M. Ivnitski
  • Glenn R. Johnson
  • Heather R. Luckarift
  • Plamen Atanassov

Organizations

  • University of New Mexico

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Air Force
  • Air Force Facilities
  • Air Force Research Laboratories
  • Amino Acids
  • Cells
  • Chemical Synthesis
  • Chemistry
  • Electrochemistry
  • Electrodes
  • Electron Transfer
  • Engineering
  • Films
  • Fungi
  • Materials
  • Measurement
  • New Mexico
  • Nuclear Engineering

Readers

  • Electrochemical Surface Science
  • Organic Chemistry

Technology Areas

  • Biotechnology
  • Microelectronics
  • Microelectronics - Graphene