Microencapsulation of Self-healing Concrete Properties

Abstract

Recent studies in the literature have demonstrated the ability of self-healing processes to be effective in enhancing the overall life of concrete. The main goal of this project is to evaluate and to control specific parameters for the production of an effective self-healing matrix that can be utilized within the application of self-healing concrete. Therefore, the project objective is to synthesize microcapsules using dicyclopentadine and sodium silicate and to evaluate the effects of pH, temperature, and agitation rate on microcapsule morphology. The microcapsule diameter, yield analysis, and shell thickness were characterized using scanning electron microscopy. During the experimental analysis, it was determined that temperature possesses a direct relationship with the pH for both sodium silicate and DCDP. As the temperature increased during the trials, the pH decreased. Temperature had a direct impact on the forming of the wall and core during the interfacial polymerization phase. Although the ability to maintain this consistency with the pH is important and essential, agitation rate is the key factor that controls the microcapsule capsule diameter size.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 2012
Accession Number
ADA567701

Entities

People

  • James Gilford Iii

Organizations

  • Louisiana State University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Alkenes
  • Chemical Synthesis
  • Chemistry
  • Civil Engineering
  • Composite Materials
  • Construction
  • Construction Materials
  • Electron Microscopy
  • Encapsulation
  • Material Degradation Processes
  • Materials
  • Materials Laboratories
  • Materials Science
  • Mechanics
  • Microcapsules
  • Microscopy
  • Scanning Electron Microscopy

Readers

  • Computer Networking
  • Mathematics or Statistics
  • Polymer Science and Technology

Technology Areas

  • Microelectronics