The Hydrophobicity and Adhesion of Heterogeneous Surfaces of Dual Nanometer and Micron Scale Structures

Abstract

An investigation was performed to study the effect a heterogeneous surface consisting of nanometer scale square posts patterned into micron scale checkerboard shapes had on surface hydrophobicity and water adhesion. In addition to altering surface geometries, different surface coatings were investigated. Conformal thin films of PDMS, CYTOP, and Teflon AF were made using a surface grafting technique and applied to each nano-scale and micro-scale design fabricated for this study. Both the static contact angle and the tilt angle required for a water drop to roll-off the surface were measured to determine the wetting state for a particular surface geometry. For nano-scale posts with spacing-to-width ratios below a certain threshold value, patterned into micro-scale checkerboard shapes with a spacing-to-width ratio <- I, the hydrophobicity of a surface was increased compared to a surface made of either all nano-scale features or all micro-scale features. Conversely, as the spacing-to-width ratio of the nano-scale square posts increased above the threshold value, for the micro-scale checkerboard shapes having a spacing-to-width ratio 5: I the surface hydrophobicity was reduced and water adhesion increased compared to a surface made of either all nano-scale features or all micro-scale features. The nano-scale spacing-to-width ratio threshold value that caused this behavior to occur was dependent on both post width and surface coating. Finally it was observed, that for the micro-scale checkerboard shapes having a spacing-to-width > 1, the micro-scale features dominated the wetting state regardless of the nano-scale post geometry.

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Document Details

Document Type
Technical Report
Publication Date
Apr 11, 2011
Accession Number
ADA570531

Entities

People

  • Alberto Cabral
  • Lalitha Parameswaran
  • Shaun Berry
  • Theodore Fedynyshyn

Organizations

  • Massachusetts Institute of Technology

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Air Force
  • Chemical Vapor Deposition
  • Coatings
  • Electron Microscopes
  • Electron Microscopy
  • Equations
  • Films
  • Geometry
  • Hydrophobic Properties
  • Materials
  • Measurement
  • Microscopy
  • Scanning Electron Microscopes
  • Scanning Electron Microscopy
  • Surface Energy
  • Thin Films
  • United States Government

Readers

  • Mathematics or Statistics
  • Nanoscale Plasmonic Nanotechnology
  • Surface Coatings Technology.

Technology Areas

  • Space