Metal Ion Sensor with Catalytic DNA in a Nanofluidic Intelligent Processor

Abstract

Due to the numerous toxicological effects of lead, its presence in the environment needs to be effectively monitored. Incorporating a biosensing element within a microfluidic platform enables rapid and reliable determinations of lead at trace levels. This work pro-duced a microchip-based lead sensor that employs a lead-specific DNAzyme (also called catalytic DNA or deoxyribozyme) as a recognition element that cleaves its complementary substrate DNA strand only in the presence of cationic lead (Pb2+). Fluorescent tags on the DNAzyme translate the cleavage events to measurable, optical signals proportional to Pb2+ concentration. The DNAzyme responds sensitively and selectively to Pb2+, and immobilizing the DNAzyme in the sensor permits both sensor regeneration and lo-calization of the detection zone. The immobilized DNAzyme retains its Pb2+ detection activity in the microfluidic device and can be regenerated and reused. The particular DNAzyme shows no response to other common metal cations and the presence of these con-taminants does not interfere with the lead-induced fluorescence signal. Attempts were made to incorporate a second DNAzyme with selectivity for uranium in the same microfluidic chip sensor, to demonstrate multiplexing capabilities for multiple metal analytes in a single injection. Crosstalk between the lead DNAzyme and the uranium DNAzyme severely limited the utility of this multi-analytic chip.

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 2011
Accession Number
ADA575220

Entities

People

  • Donald M. Cropek
  • Jonathan V. Sweedler
  • Mark A. Shannon
  • Paul Bohn
  • Tulika S. Dalavoy
  • Yi Lu

Organizations

  • Engineer Research and Development Center

Tags

Communities of Interest

  • Biomedical
  • Ground and Sea Platforms
  • Sensors

DTIC Thesaurus Topics

  • Buffers (Chemistry)
  • Chemical Analysis
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Detection
  • Detectors
  • Environment
  • Environmental Protection
  • Hydroxides
  • Liquid Chromatography
  • Mass Spectrometry
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Organic Chemistry
  • Three Dimensional

Fields of Study

  • Chemistry

Readers

  • Integrated Circuit Design and Technology.
  • Nanoscale Plasmonic Nanotechnology
  • Underwater engineering and Marine Technology.