Terminating Platinum-Initiated Cation-Olefin Reactions with Simple Alkenes

Abstract

The en masse cyclization of polyolefins into polycyclic terpenoids by cyclase enzymes (e.g. squalene to hopene), is a biosynthetic reaction of particular fascination to chemists. Noteworthy recent additions to synthetic mimics of the cyclase enzymes are asymmetric methods that include Br nsted Lewis acids (BLA), masked equivalents of Br+ and I+, organocatalysts, and electrophilic metal catalysts. With the exception of HgII reagents, few electrophilic metal catalysts cyclize polyenes with bio-like alkene terminators. The development of methods whose catalysts can initiate, cyclize, and terminate polyenes under ligand control would significantly advance the state of the art.

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Document Details

Document Type
Technical Report
Publication Date
May 05, 2011
Accession Number
ADA579557

Entities

People

  • Chandra S. Korapala
  • Jennifer J. Becker
  • Joseph G. Sokol
  • Michel R Gagné
  • Peter S. White

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Biomedical
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Acids
  • Catalysts
  • Chemical Kinetics
  • Chemical Synthesis
  • Chemistry
  • Column Chromatography
  • Contrast
  • Energy
  • Geometry
  • Heat Of Activation
  • Lewis Acids
  • Military Research
  • New York
  • North Carolina
  • Platinum
  • Single Crystals
  • X Rays

Fields of Study

  • Chemistry

Readers

  • Organic Chemistry