Incremental Sampling Methodology (ISM) for Metallic Residues

Abstract

Heterogeneous distribution of metallic residues in surface soils creates unique challenges for collecting soil samples that provide representative and reproducible results. In particular, soils containing metal fragments at military training ranges, such as small-arms ranges, are especially problematic to analyze owing to their large compositional and distributional (i.e., spatial) heterogeneities. The recognition of the heterogeneous nature of energetic residues in surface soils at military training ranges resulted in significant changes to the field sampling and sample processing procedures for energetics as described in United States Environmental Protection Agency (USPEA) SW-846 Method 8330B. The incremental sampling methodology (ISM) of Method 8330B for energetics was modified to develop a similar approach for metals. The approach has been successfully implemented to analyze surface soils with metallic residues at several active and inactive military training ranges. In most cases, ISM produced results more representative and reproducible than results from conventional grab (i.e., discrete) sampling and analysis procedures for surface soils collected from small-arms ranges containing metallic residues.

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Document Details

Document Type
Technical Report
Publication Date
Aug 01, 2013
Accession Number
ADA585469

Entities

People

  • Anthony Bednar
  • Jay L. Clausen
  • Thomas Georgian

Organizations

  • Cold Regions Research and Engineering Laboratory

Tags

Communities of Interest

  • Biomedical
  • Ground and Sea Platforms
  • Weapons Technologies

DTIC Thesaurus Topics

  • Chemical Synthesis
  • Chemistry
  • Department Of Defense
  • Ecology
  • Environmental Protection
  • Explosives
  • Hydroxides
  • Liquid Chromatography
  • Military Training
  • Particle Size
  • Sampling
  • Small Arms
  • Test Methods
  • Training
  • United States
  • Water
  • Water Resources

Readers

  • Distributed Systems and Data Platform Development
  • Environmental Remediation and Restoration.
  • Nanoscale Plasmonic Nanotechnology