Inkjet Assisted Creation of Self-Healing Layers Between Composite Plies

Abstract

This project aimed to design and optimize a novel composite system using self-healing agent deposited in microscopically-ordered arrays through ink-jet printing, to arrest cracks along interfaces between composite plies. Novel aspects included the method itself, the highly-controlled crack arrest mechanism provided by self-healing microdroplets between plies, and the ability to rapidly transfer this technology into a prepreg manufacturing process. The approach consisted of depositing novel thermoplastic low-viscosity microdroplets with chemically and mechanically comparable properties to epoxy matrix in aerospace grade composites onto fiber-reinforced epoxy prepregs before curing using an ink-jet system. The report focuses on the most successful configuration using poly(methyl methacrylate) (PMMA) on Boeing-accredited toughened carbon fiber epoxy prepreg Cycom977-2. Double cantilever beam (DCB) and short beam shear (SBS) tests were used to evaluate the self-healing efficiency. It was shown that carefully selected printed self-healing agents increased both shear modulus and fracture toughness simultaneously, without imparting any parasitic weight, and restored the properties of the damaged and self-healed composite to a large degree following post-damage heat treatment. A patent application has been submitted by the University of Sheffield.

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Document Details

Document Type
Technical Report
Publication Date
Jul 29, 2013
Accession Number
ADA587429

Entities

People

  • Alma Hodzic
  • Patrick T Smith

Organizations

  • University of Sheffield

Tags

Communities of Interest

  • Space

DTIC Thesaurus Topics

  • Advanced Manufacturing
  • Air Force Research Laboratories
  • Alkenes
  • Cantilever Beams
  • Carbon Fibers
  • Composite Materials
  • Efficiency
  • Fibers
  • Heat Treatment
  • Inks
  • Manufacturing
  • Materials
  • Materials Science
  • Optical Images
  • Patent Applications
  • Patents
  • Shear Modulus

Fields of Study

  • Materials science

Readers

  • Materials Science (Mechanical Engineering).
  • Nanofabrication and Microfabrication.
  • Reinforced Composite Materials

Technology Areas

  • Space