Reversible Tailoring of Mechanical Properties of Carbon Nanotube Forests by Immersing in Solvents

Abstract

The mechanical behavior of carbon nanotube (CNT) forests soaked in three solvents toluene, acetonitrile, and isopropanol is examined. Effective stiffness of the structure is evaluated in the dry and wet condition by micro-indentation using a 100 lm flat punch. With soaking of CNT forests in solvents, the stiffness decreases and deformation mechanism changes from buckling concentrated close to the bottom of the CNT forest to a distribution of local buckles along the height and global buckling of the entire length of CNTs. We use molecular dynamics simulations to relate the experimental observations to the reduced mechanical support from neighbor CNTs due to a decreased magnitude of van derWaals (vdW) interactions in the presence of solvents. Toluene, which produces the lowest average measured stiffness between the three solvents, produces the lowest vdW forces between individual CNTs. Furthermore, wet-dry cycling of CNT forests shows the reversibility and repeatability of change of stiffness by immersing in solvents. The results show that soaking CNT forests in solvents could be useful for applications such as interface materials where lower stiffness of CNT forests are needed and applications such as energy absorbing materials in which re-setting of stiffness is required.

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Document Details

Document Type
Technical Report
Publication Date
Dec 07, 2014
Accession Number
ADA600900

Entities

People

  • Baratunde A. Cola
  • Jeffery W Baur
  • Matthew R Maschmann
  • Parisa P. Abadi
  • S. M. Mortuza
  • Samuel Graham
  • Soumik Banerjee

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Air Force
  • Carbon Nanotubes
  • Carbon-Based Paper
  • Chemical Vapor Deposition
  • Chemistry
  • Fullerenes
  • Materials
  • Materials Engineering
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Mechanical Engineering
  • Mechanical Properties
  • Mechanics
  • Modulus Of Elasticity
  • Molecular Dynamics
  • Simulations

Readers

  • Forest Ecology
  • Nanocomposite Materials Science
  • Structural Dynamics.