Development of Antimicrobial Coatings by Atmospheric Pressure Plasma Using a Guanidine-Based Precursor

Abstract

Antimicrobial coatings deposited onto ultra high molecular weight polyethylene (UHMWPE) films were investigated using an atmospheric pressure plasma enhanced chemical vapor deposition (AP-PECVD) process. Varying concentrations of a guanidine-based liquid precursor, 1,1,3,3-tetramethylguanidine, were used, and different deposition conditions were studied. Attenuated total reflectance Fourier Transform Infrared (ATR-FTIR) spectroscopy and X-ray Photoelectron Spectroscopy (XPS) were used to study the chemical structure and elemental composition of the coatings. Conformity, morphology, and coating thickness were assessed through SEM and AFM. Optimal AP-PECVD parameters were chosen and applied to deposit guanidine coatings onto woven fabrics. The coatings exhibited high antimicrobial activity against Escherichia coli (E. coli) and Staphylococcus aureus (S. aureus) based on a modified-AATCC 100 test standard, where 2 5 log reductions were achieved.

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Document Details

Document Type
Technical Report
Publication Date
Oct 29, 2013
Accession Number
ADA608004

Entities

People

  • Andre A. Williams
  • Daphne D. Pappas
  • Jacqueline H. Yim
  • Julia L. Leadore
  • Lars T. Piehler
  • Michelle S. Fleischman
  • Victor Rodriguez-santiago

Organizations

  • United States Army Research Laboratory

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Anti-Infective Agents
  • Barometric Pressure
  • Chemical Vapor Deposition
  • Chemistry
  • Coatings
  • Materials
  • Materials Processing
  • Materials Science
  • Molecules
  • Physical Properties
  • Polyethylenes
  • Polymers
  • Spectra
  • Spectroscopy
  • Surface Roughness
  • Vapor Deposition
  • X Ray Photoelectron Spectroscopy

Fields of Study

  • Materials science

Readers

  • Microbial Pathology
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene