New Approaches to Maximizing Thermo-oxidation Resistance of Polycyanurate Networks

Abstract

Among thermosetting resins, polycyanurate networks (derived from cyanate ester monomers) offer excellent flame, smoke, and toxicity characteristics along with enhanced thermo-oxidative stability compared to epoxy resins. Recent structure-property investigations in polycyanurate networks have revealed new insights into the relationship between the chemical moieties found in the networks and the corresponding levels of thermo-oxidative resistance. In particular, it appears that the presence of methyl groups next to tertiary or quaternary carbons has a decidedly negative impact on thermo-oxidative stability during TGA heating ramp tests. In the case of silicon-containing cyanate esters, thermo-oxidative stability can be improved significantly by the incorporation of silicon only in cases where either a large portion of the chemical repeat unit is formed from inorganic groups, or the thermo-oxidative stability of the carbon-containing analog is relatively poor compared to other organic polycyanurate networks.

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Document Details

Document Type
Technical Report
Publication Date
Aug 13, 2014
Accession Number
ADA621044

Entities

People

  • Andrew J. Guenthner
  • Gregory R. Yandek
  • Joseph M Mabry
  • Josiah T. Reams
  • Kevin R. Lamison
  • Matthew C. Davis
  • Timothy S. Haddad
  • Vandana Vij

Organizations

  • Air Force Research Laboratory

Tags

Communities of Interest

  • Weapons Technologies

DTIC Thesaurus Topics

  • Air Force
  • Air Force Research Laboratories
  • Chemical Stability
  • Department Of Defense
  • Epoxy Resins
  • Fires
  • Glass Transition Temperature
  • Governments
  • Materials
  • Oxidation Resistance
  • Plastics
  • Polymers
  • Resins
  • Resistance
  • Rigid Rod Polymers
  • Thermosetting Plastics
  • Transition Temperature

Fields of Study

  • Materials science

Readers

  • Polymer Science and Engineering.