Development of High Temperature Addition-Cured Adhesives

Abstract

An evaluation of two high-temperature addition-cured adhesives. These were (1) NITRILE SUBSTITUTED POLYPHENYL ETHERS CURED WITH TERPHTHALONITRILE N, N-dioxide (TPNO) AND (2) acetylene termin-ated polyimide (HR600) cured thermally. The thermally cured acetylene terminated polyimide proved to be superior to the TPNO cured cyano substituted polyphenylene oxide. Lap-shear strengths of 6A14V titanium bonded with HR600 adhesive exceeded 3000 psi at ambient temperature on powdered aluminum-filled specimens reinforced with heat cleaned 112 glass fabric and 2800 psi at ambient temperature, 2600 psi at 450^F and 2100 psi at 500^F on unfilled specimens bonded with 70 percent HR600 prepreg on 112 heat cleaned glass fabric. Weld-bonding of titanium specimens using aluminum powder filled HR600 adhesive proved to be successful and showed superior fatigue resistance over spot-welded specimens.

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Document Details

Document Type
Technical Report
Publication Date
May 01, 1974
Accession Number
ADB000277

Entities

People

  • H. Raech
  • Norman Bilow
  • Robert H. Boschan

Organizations

  • Hughes Aircraft Company

Tags

Communities of Interest

  • Air Platforms

DTIC Thesaurus Topics

  • Air Force
  • Aircrafts
  • Anhydrides
  • Composite Materials
  • Failure Mode And Effect Analysis
  • Fatigue Tests (Mechanics)
  • Heat Energy
  • High Temperature
  • Infrared Spectra
  • Materials
  • Materials Laboratories
  • Materials Testing
  • Resistance
  • Shear Strength
  • Shear Tests
  • Test And Evaluation
  • Titanium

Fields of Study

  • Materials science

Readers

  • Metallurgy
  • Polymer Science and Engineering.