Preparation of 1,3,5,7 Tetracetamido - and 1,3,5,7 -Tetraaminodamantanes.
Abstract
1,3,5,7 - Tetraacetamidoadamantane is prepared by reacting 1,3,5,7 - tetraiodoadamantane with acetonitrile and water in the presence of actinic radiation. The 1,3,5,7 - tetraacetamidoadamantane can be hydrolyzed with hydrochloric acid to produce 1,3,5,7 - tetraaminoadamantane tetrahydrochloride, which can be converted to the free base by treatment with an equivalent amount of an alkali, e.g. aqueous sodium hydroxide. (Author)
Document Details
- Document Type
- Technical Report
- Publication Date
- Jul 10, 1980
- Accession Number
- ADD007813
Entities
People
- Gilbert P. Sollott
Organizations
- United States Army