Preparation of Steel Surfaces for Adhesive Bonding.

Abstract

A principal object of the present invention is to provide a novel process and composition for etching steel, which avoids the use of ethanol solvent with phosphoric acid yet produces a steel surface which, when adhesively bonded, yields joints of comparable strength and stress durability to those obtained by use of the phosphoric acid-ethanol etchant. According to the present invention the foregoing and other objects can be achieved by contacting the steel parts with an etchant composition consisting essentially of phosphoric acid and a liquid polyhydric alcohol, particularly a didhydric and/or trihydric alcohol. Exemplary polyhydric alcohols suitable for use in the process and compositions of the present invention include ethylene-glycol, dietryleneglycol, triethylene glycol, polyethylene glycol 400, 1,2- and 1,3- propylene glycol, 1,4- butanediol and glycerine.

Document Details

Document Type
Technical Report
Publication Date
Jun 24, 1982
Accession Number
ADD009820

Entities

People

  • Roberta Rosty
  • William J. Russell

Organizations

  • United States Army

Tags

Communities of Interest

  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Acids
  • Adhesive Bonding
  • Adhesives
  • Alcohols
  • Alkenes
  • Ethylene Glycol
  • Ethylenes
  • Glycols
  • Inventions
  • Phosphoric Acids
  • Polyethylene Glycols
  • Propenes
  • Propylene Glycol

Readers

  • Polymer Science and Engineering.
  • Surface Coatings Technology.