In-Situ Monitoring and Feedback Control of Metalorganic Precursor Delivery.

Abstract

The in-situ monitoring of metalorganic precursor delivery in a metalorganic chemical vapor deposition oxide system in high temperature super conductors (HTSC) film growth is accomplished by utilizing the distinct absorbance bands for metalorganic compounds. As an ultraviolet-visible light beam is passed through an effluent metalorganic gas stream the relative change in ultraviolet-visible absorbance of the ultraviolet-visible light beam passing through the effluent metalorganic gas stream is monitored. Stoichiometry control is achieved by feeding back absorbance data to a controlling parameter such as carrier gas mass flow rate, thus stabilizing fluctuations in source concentration in the bubble effluent from a computer or similar monitoring device. Such an apparatus and method improves the stoichiometry control of mixed metal oxide film deposition and increases the manufacturability of thin films.

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Document Details

Document Type
Technical Report
Publication Date
Oct 06, 1995
Accession Number
ADD018186

Entities

People

  • Brian Rappoli
  • William J. Desisto

Organizations

  • United States Department of the Navy

Tags

Communities of Interest

  • Advanced Electronics
  • Sensors

DTIC Thesaurus Topics

  • Chemical Vapor Deposition
  • Films
  • Flow
  • Flow Rate
  • High Temperature
  • Mass Flow
  • Materials
  • Measurement
  • Metal Oxides
  • Oxide Films
  • Oxides
  • Partial Pressure
  • Spectra
  • Spectroscopy
  • Thin Films
  • Vapor Deposition
  • Visible Spectra

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Emergency Management and Homeland Security.
  • Geodesy