Application of Metal Alkoxides in the Synthesis of Oxides,

Abstract

Powders and thin films of the following simple and complex oxides have been obtained from metal alkoxides: M(11)TiO3 (M=Mg, Ca-Ba), MM1/3B2/3O3 (M=Sr,Ba,M'=Mg-Zn; B=Nb,Ta); MNbO3(M=Li,Na); ZrTiO4; PbTiO3; PST, PLZT-materials; M2BO4 (M=Li,Na; B=Mo,W), Bi2BO6(B=Mo,W); Li sub x WO3, WO3, MoO3, Bi2O3-WO3(solid solutions), YFeO3,Y3Fe5O12; YBa2Cu3O7-x; Bi2Sr2CaCu2Ox; Bi2Sr2Ca2Cu3Ox. For synthesis of metal alkoxides and solutions containing two or more elements electrochemical technique (the anodic dissolution of metals in alcohols) has been used. Analysis of different examples emphasises that considerable attention in sol-gel chemistry of oxides should be paid to decomposition of M(OR)n with elimination of ether and formation of oxoalkoxides, containing M-0-M' bonds - the basis of future oxide phases.

Document Details

Document Type
Technical Report
Publication Date
Apr 05, 1991
Accession Number
ADP006653

Entities

People

  • E. P. Turevskaya
  • M. I. Yanovskaya
  • V. G. Kessler

Organizations

  • Karpov Institute of Physical Chemistry

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Chemistry
  • Colorado
  • Decomposition
  • Elimination
  • Films
  • Materials
  • Materials Science
  • Physics
  • Solid Solutions
  • Thick Films
  • Thin Films

Fields of Study

  • Chemistry
  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Military Logistics and Supply Chain Management
  • Surface Engineering/Surface Coating Technology.