The Effects of Charge Separation in Quaternary Ammonium, DABCO-Containing Polymers on In Vitro Toxicity and Gene Delivery

Abstract

Polycation materials have recently emerged as promising systems for the delivery of genetic material. In this study, several DABCO (1,4-diazabicyclo2.2.2octane) polymers are investigated for their ability to bind and deliver plasmid DNA (pDNA) into mammalian cells. The DABCO polymers are synthesized by copolymerization of DABCO with 1,3- dibromopropane (D3), 1,4-dibromobutane (D4), 1,6-dibromohexane (D6), 1,8-dibromooctane (D8), and 1,10-dibromodecane (D10) to form a series of quaternary ammonium polymers with increasing charge separation. Gel retardation experiments reveal that each polymer (D3-D10) binds pDNA above a charge ratio of 1.0 (polymer + /pDNA -). The polycations are examined for in vitro transfection efficiency and toxicity in BHK-21 cells. Results of the transfection experiments indicate that the D6 polymer had the highest transfection efficiency. Although all of the polymers are shown to have some toxicity, the D8 and D10 polymers are more toxic to BHK- 21 cells; approximately 30% of the cells survive at a charge ratio of 5 +/- as compared to the D3, D4, and D6 polymers where survival rates are about 80%.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
Apr 01, 2002
Accession Number
ADP014421

Entities

People

  • Mark E. Davis
  • Theresa M. Reineke

Organizations

  • California Institute of Technology

Tags

DTIC Thesaurus Topics

  • Cell Line
  • Cell Physiological Processes
  • Cells
  • Chemical Compounds
  • Chemical Engineering
  • Chemical Synthesis
  • Chemistry
  • Culture Techniques
  • Cultured Cells
  • Efficiency
  • Gel Electrophoresis
  • Gene Delivery
  • Light Scattering
  • Materials
  • Methylenes
  • Molecular Weight
  • Polymerization

Fields of Study

  • Chemistry

Readers

  • Molecular Genetics
  • Polymer Science and Technology

Technology Areas

  • Biotechnology
  • Biotechnology - Cancer Biotech