Processing and Development of Nano-Scale HA Coatings for Biomedical Application

Abstract

Functionally graded Hydroxyapatite coating with graded Crystallinity across the thickness of the film has been processed and tested as a more effective orthopedic/dental implant coating. The present study aims to increase the service-life of an orthopedic/dental implant by creating materials that form a strong, long lasting, bond with the Ti substrate as well as juxtaposed bone. The health relatedness of the new material is to increase bonding between an implant and juxtaposed bone so that a patient who has received joint or dental replacement surgery may quickly return to a normal active lifestyle. Cross-sectional transmission electron microscopy analysis displayed that the films have a graded crystal structure with the crystalline layer near the substrate and the amorphous layer at the top surface. Compositional analysis was performed using SEM-EDX at the top surface as wee as STEM-EDX at the cross section of the film. The average calcium to phosphorous ratio at the surface is 1.46 obtained SEM-EDX. The Ca/P ratios in the crystalline and amorphous layers of the film are 1.6 to 1.7, close to the ratio of 1.67 for HA.

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Document Details

Document Type
Technical Report
Publication Date
Jan 01, 2005
Accession Number
ADP019720

Entities

People

  • Afsaneh Rabiei
  • Brent Thomas

Organizations

  • North Carolina State University

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Chemical Compounds
  • Coatings
  • Crystal Structure
  • Crystals
  • Deposition (Materials Processing)
  • Electron Microscopes
  • Elements
  • Films
  • Heat Treatment
  • Ion Beams
  • Ion Sources
  • Materials
  • Materials Science
  • Metals
  • Microscopes
  • Prosthetics
  • Scanning Electron Microscopes

Fields of Study

  • Materials science

Readers

  • Thin Film Deposition Science.
  • Virology (or Medical Virology).

Technology Areas

  • Biotechnology
  • Microelectronics
  • Microelectronics - Graphene