In Situ Liquid Cell TEM Holder for Characterizing Dynamic Behavior of Materials in Liquid Environments

Abstract

This proposal is for the acquisition of an in situ liquid cell specimen holder to enable transmissionelectron microscopy (TEM) in liquid or gaseous environments. TEM is the primary method forobserving structure and chemistry of materials at the atomic scale, but conventional TEM requiresa vacuum environment. The in situ liquid cell holder proposed for purchase (the Poseidon Selectmodel manufactured by Protochips, Inc.) features a liquid layer encapsulated by electrontransparentwindows, and it allows for the observation of materials behavior in liquids that can becontrollably flowed through the chamber. It also features electrical biasing and heatingcapabilities, which enable the investigation of electrochemical phenomena and materials synthesisin the liquid phase. This in situ holder is the final piece that is needed to complete Georgia Tech’sin situ TEM suite, which features multiple novel imaging and data processing modalities inconjunction with other in situ holders that allow for electrical biasing, heating, and mechanicaldeformation in vacuum environments.

Document Details

Document Type
DoD Grant Award
Publication Date
Jul 24, 2019
Source ID
FA95501810509

Entities

People

  • Matthew T McDowell

Organizations

  • Air Force Office of Scientific Research
  • Georgia Tech Research Corporation
  • United States Air Force

Tags

Readers

  • Combustion and Flow Dynamics.
  • Distributed Systems and Data Platform Development
  • Nanoscale Plasmonic Nanotechnology