Protein-Polymer Bioconjugate Structures Measured by Magnetic Resonance

Abstract

Protein-polymer conjugates provide an opportunity to stabilize proteins for challenging environments. The soldier will likely encounter such challenging environments in the field. These polymer stabilized proteins present capabilities that can be utilized for the detection of chemical or biological agents. Rational design of stabilized protein-polymer conjugates requires an understanding of the design rules that govern bioconjugate performance. Unfortunately, these design rules have eluded the field, with conflicting mechanisms of stabilization reported. The proposed research will develop nuclear magnetic resonance spectroscopy techniques for determining the interactions present between the synthetic macromolecule and protein within a protein-polymer bioconjugates. We will pair precision polymer synthesis with advanced nuclear magnetic resonance methods for protein structure determination to define the structure of protein-polymer conjugate at atomic resolution. When correlated with bioconjugate activity and stability, the technique will enable the extraction of design rules that can be used to produce improved protein-polymer conjugates, which can perform in harsh and challenging environments.

Document Details

Document Type
DoD Grant Award
Publication Date
May 28, 2019
Source ID
W911NF1910300

Entities

People

  • Dominik Konkolewicz

Organizations

  • Army Contracting Command
  • Miami University
  • United States Army

Tags

Readers

  • Molecular and Cellular Biochemistry
  • Nanocomposite Materials Science