RESEARCH ON THE BEHAVIOR OF NEARLY PERFECT CRYSTALS

Abstract

Etching techniques have been developed which are capable of producing etch pits at the intersection of dislocation lines with various crystal surfaces of high-purity single crystals of alpha-iron. For the (100) and (110) surfaces, dislocations can be revealed with or without the segregation of a specific impurity to the dislocation sites. Similar etching reagents can be used to reveal dislocations on the (110), (112) and (491) surfaces as well as all surfaces that make an angle of more than 5 degrees with the (100) and (111) planes. The dislocation structure of selected iron whiskers with (100), (110), and (111) growth axes was evaluated using the above etching techniques. There was some qualitative indication that the perfection of the whiskers increases with decrease in whisker diameter and with increase in purity of the halide salt used in their growth.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1961
Accession Number
AD0265522

Entities

People

  • Paul D. Gorsuch
  • Thomas H. Alden

Organizations

  • General Electric

Tags

Communities of Interest

  • Air Platforms

DTIC Thesaurus Topics

  • Air Force
  • Alcohols
  • Chemistry
  • Crystals
  • Diameters
  • Electron Microscopy
  • Geometry
  • Hydrochloric Acid
  • Impurities
  • Line Defects
  • Low Angles
  • Material Degradation Processes
  • Mechanical Properties
  • Methanols
  • Microscopes
  • Microscopy
  • Single Crystals

Fields of Study

  • Materials science

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Nanofabrication and Microfabrication.
  • Powder metallurgy of Titanium alloys.