Preparation of Analytically Pure Monobasic Copper Salicylate
Abstract
Preparation of analytically pure monobasic copper salicylate by two distinct synthetic routes and characterization of the products by infrared spectroscopy, X-ray diffraction and thermogravimetric analysis is described. Analytically pure monobasic copper salicylate can be synthesized in excellent yield by reacting basic copper carbonate and salicylic acid in a 1 to 2.2 molar ratio. The pure monobasic salt can also be prepared by reacting copper hydroxide and salicylic acid in a 1 to 1 molar ratio. However, the yield, in this case, is comparatively low, Characterization of the product can be accomplished by infrared spectroscopy, X-ray diffraction, thermogravimetric analysis, and elemental analysis for copper, carbon and hydrogen.
Document Details
- Document Type
- Technical Report
- Publication Date
- Oct 01, 1971
- Accession Number
- AD0732352
Entities
People
- Daniel R. Satriana
Organizations
- Picatinny Arsenal