Bioelectrocatalyzed Nitrogen Fixation under Standard Conditions

Abstract

Report developed under topic A13A-T007, contract W911NF-14-C0162. This final report describes the development of a bioelectrocatalyzed nitrogen fixation process using algae biofilm electrodes. The Phase II effort included: Algae biofilm testing of lifetime and robustness, isolation and investigation of nitrogenase, nitrite/nitrate reductase enzymes, electrochemical stimulation of algae, electrolyte concentration and cation identity, process scale-up, ammonia separation, in-situ ammonia generation, studies on the nitrogen fixation method in algae including modelling and cost modelling of the process. The process achieved 16 uM ammonia at 8% coulombic efficiency in a 400mL volume. Ammonia separation without additional chemicals reached >90% efficiency. The process was scaled from 20 cm2 to 200 cm2.Results suggest that the process is viable for a small-scale industrial process, tons/day, with further improvements. Potential applications include distributed commodity chemical manufacturing for fuel, propellants and fertilizer.

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Document Details

Document Type
Technical Report
Publication Date
Nov 07, 2016
Accession Number
AD1038463

Entities

People

  • John Watkins

Tags

Communities of Interest

  • Energy and Power Technologies

DTIC Thesaurus Topics

  • Amines
  • Buffers (Chemistry)
  • Cell Membrane
  • Chemical Synthesis
  • Chemistry
  • Electrochemical Reactions
  • Hydroxides
  • Materials
  • Materials Processing
  • Materials Science
  • Nitrogen Compounds
  • Nitrogen Oxides
  • Organic Chemistry
  • Oxidation Reduction Reactions
  • Rocket Oxidizers

Readers

  • Electrochemical Engineering/ Fuel Cell Technologies
  • Environmental Engineering.
  • Microbial Pathology

Technology Areas

  • Biotechnology
  • Biotechnology - Bioremediation