Fabrication of Complex-Shaped Ceramic Components by Room-Temperature Injection Molding of Ceramic Suspension Gels

Abstract

Novel forming of ceramics into complex shapes of silicon nitride (Si3N4) and boron carbide (B4C) has been investigated. Common to our approach was to use a polymer in the ceramic-loaded suspensions. The polymer employed was flowable at room-temperature, water soluble, imparted green strength to the formed body, and in some cases, acted as a dispersing agent. Lisa Rueschhoff developed suspensions of silicon nitride powders. She was able to show that that water reducing admixtures used in concrete are effective for dispersing Si3N4 in water. These suspensions have been injection molded. Andres Diaz Cano has investigated preparation of aqueous suspensions of boron carbide powders, achieving up to 56 vol. percent B4C powder loadings. He has also studied the best sintering aids to density B4C without external pressure at low temperatures (2000 deg C). We were fortunate enough to win both a URAP and HRAP awards for the summer of 2015. In this work, we developed suspensions of alumina (Al2O3) and boron carbide, and used a syringe-style additive manufacturing approach to print complex shapes. William Costakis was the undergraduate awardee, while Alycia McEachen was the high student student awardee. As a team they were very successful using a 3D printing process to make B4C parts.

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Document Details

Document Type
Technical Report
Publication Date
Nov 29, 2016
Accession Number
AD1063246

Entities

People

  • Jeffrey P Youngblood
  • Rodney W. Trice

Organizations

  • Purdue University

Tags

Communities of Interest

  • Advanced Electronics

DTIC Thesaurus Topics

  • Additive Manufacturing
  • Ceramic Materials
  • Chemistry
  • Fabrication
  • Flexural Strength
  • Geometry
  • Manufacturing
  • Materials
  • Materials Engineering
  • Materials Processing
  • Materials Science
  • Mechanical Properties
  • Mechanical Working
  • Shear Stresses
  • Students
  • Three Dimensional
  • Turbines

Fields of Study

  • Materials science

Readers

  • Military History
  • Nanocomposite Materials Science
  • Powder metallurgy of Titanium alloys.