Engineering Superhydrophobic Behavior in 3D-Printed Stainless Steel Composites

Abstract

This thesis discusses the wettability of 316L stainless steel composites using carbon nanotubes and manufactured via a selective laser melting. Superhydrophobicity is created through the combination of low surface tension and surface roughness at a micro to nanoscopic scale, and it has become a topic of vigorous study over the past 20 years. Previous studies have relied primarily on processes such as etching and nanomaterial arrays to generate surface roughness, followed by the application of harmful chemicals (e.g.,fluorosilanes) to modify surface energy and achieve superhydrophobicity. Stainless steel powder (316L) was combined with carbon nanotubes, which demonstrate near-hydrophobic properties, via high energy ball milling in attempts to reduce the materials surface energy. An ideal pillared surface geometry based on natural superhydrophobicity was produced through additive manufacturing using multiple concentrations of carbon nanotube composites. Through material characterization including sessile water drop contact angle measurements, optical profilometry, and microscopy, it was determined that all samples remained hydrophilic in nature due to insufficient surface energy modification using carbon nanotubes. However, trends indicate that further increasing CNT concentration, controlling printing laser energy density, and slight model modifications could demonstrate hydrophobic effects.

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Document Details

Document Type
Technical Report
Publication Date
Jun 01, 2022
Accession Number
AD1184804

Entities

People

  • Justin M. Budan

Organizations

  • Naval Postgraduate School

Tags

Communities of Interest

  • Advanced Electronics
  • Biomedical
  • Energy and Power Technologies
  • Ground and Sea Platforms

DTIC Thesaurus Topics

  • Additive Manufacturing
  • Ball Mills
  • Carbon Nanotubes
  • Chemistry
  • Computer-Aided Design
  • Corrosion Resistance
  • Electron Microscopes
  • Fabrication
  • Finishes
  • Hydrophilic Properties
  • Hydrophobic Properties
  • Manufacturing
  • Material Degradation Processes
  • Materials
  • Materials Processing
  • Materials Science
  • Measurement
  • Selective Laser Melting
  • Selective Laser Sintering
  • Surface Roughness
  • United States

Fields of Study

  • Materials science

Readers

  • Nanocomposite Materials Science
  • Powder metallurgy of Titanium alloys.
  • Thin Film Deposition Science.

Technology Areas

  • Directed Energy