Fracture Toughness Testing of a Ceramic Matrix Composite at Elevated Temperatures

Abstract

The need for a load fixture and technique for determining the fracture toughness in fiber reinforced ceramic composites at elevated temperatures was identified. A three point bend load fixture capable of withstanding temperatures up to 1000 degrees Fahrenheit was designed and constructed. A test procedure for finding compliance and critical load at room and elevated temperatures was developed. Specimens were tested at varying crack lengths at room temperature, 600, and 1000 degrees Fahrenheit. Postmortem examination was done on specimens for each temperature. Specimens tested at 600 F had smoother Mode II fracture surfaces than the room temperature specimens including a more brittle fracture and supporting the experimental results. The specimens tested at 1000 F had a rougher Mode II fracture surface with fiber pull-out and small matrix fragments attached to the fibers indicating a more ductile failure and therefore increasing the fracture toughness. A color change from black to dark gray and the presence of crystals on the Mode I fracture surface of the 1000 F specimens indicated a chemical change in the specimens. The apparent chemical change and significantly higher fracture toughness in the material at elevated temperatures. Keywords: Military theses; Fracture mechanics; Crack propagation. (KT/JES)

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Document Details

Document Type
Technical Report
Publication Date
Dec 01, 1988
Accession Number
ADA202738

Entities

People

  • John H. Mol

Organizations

  • Air Force Institute of Technology

Tags

Communities of Interest

  • Advanced Electronics
  • Energy and Power Technologies
  • Human Systems
  • Space

DTIC Thesaurus Topics

  • Air Force
  • Ceramic Materials
  • Ceramic Matrix Composites
  • Composite Material Fabrication
  • Composite Materials
  • Failure Mode And Effect Analysis
  • Fiber Reinforced Composites
  • Fracture (Mechanics)
  • Materials
  • Materials Laboratories
  • Materials Processing
  • Materials Science
  • Materials Testing
  • Measurement
  • Mechanical Properties
  • Mechanics
  • Micromechanics

Readers

  • Reinforced Composite Materials
  • Structural Health Monitoring of Composite Structures.
  • Thermal Physics or Thermal Science.