Basic Research on Processing of Ceramics for Space Structures
Abstract
The hydrolysis of alkoxide emulsion droplets was investigated for preparing un-agglomerated, submicrometer oxide ceramic particles with a homogeneous composition. This technique was used to prepare single- and mixed- oxide powders whose overall cation composition corresponded to the initial alkoxide cation composition. Uncalcined powders were amorphous, with high surface areas and low densities; upon calcination, powders densified and became crystalline. In other studies, a water-in-oil emulsion technique was investigated for preparing SrTiO3, and two AIN precursors were synthesized from dimethylaminoalane and NH3 . Both AIN precursors gave fine, high purity AIN powders after heat-treatment a colloidally pressed sample densified to 95% of theoretical density at 1750 C. Ceramics, Composite ceramics, Cyclic annealing, Organosilicon polymeric binders, Polymer-coated SiC.
Document Details
- Document Type
- Technical Report
- Publication Date
- Jan 31, 1989
- Accession Number
- ADA205954
Entities
People
- B. A. Bishop
- H. R. Bowen
- S. Kamiya
- W. C. Moffatt
- W. E. Rhine
Organizations
- Massachusetts Institute of Technology