The Determination of Rate-Limiting Steps during Soot Formation

Abstract

A single-pulse shock tube has been used to examine toluene pyrolysis and the rich oxidation of benzene diluted in argon over the temperature range of 1200 to 2000K and at total pressures of ten to thirteen atmospheres. Dwell times were about 500 microseconds. Collected gas samples were analyzed using gas chromatography for hydrogen, carbon oxides and C1- to C14- hydrocarbons. Low molecular weight products during benzene oxidation include cyclopentadiene and vinylacetylene and support literature proposals for oxidation of benzene. High molecular weight products are dominated by species containing mixtures of five- and six- membered rings. During toluene pyrolysis very rapid production of polyaromatic hydrocarbons occurs between 1400 and 1450K, consistent with temperatures at which particle inception occurs in diffusion flames.

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Document Details

Document Type
Technical Report
Publication Date
Apr 27, 1989
Accession Number
ADA208866

Entities

People

  • D. J. Seery
  • J. J. Sangiovanni
  • M. B. Colket
  • Richard J. Hall

Organizations

  • United Technologies Corporation

Tags

Communities of Interest

  • C4I
  • Energy and Power Technologies
  • Ground and Sea Platforms
  • Materials and Manufacturing Processes

DTIC Thesaurus Topics

  • Alkenes
  • Alkynes
  • Aromatic Hydrocarbons
  • Chemical Analysis
  • Chemical Kinetics
  • Chemical Reaction Properties
  • Chemical Reactions
  • Chemical Synthesis
  • Chemistry
  • Chromatography
  • Decomposition
  • Dwell Time
  • Gas Chromatography
  • Hydrocarbons
  • Measurement
  • Organic Chemistry
  • Plastic Explosives

Fields of Study

  • Environmental science

Readers

  • Organic Chemistry
  • Plasma Physics.