Effect of Excess Oxydianiline on the Properties of Polyimide

Abstract

Thin films of the polymer polyimide (PI) can be grown in ultra-high vacuum by codeposition of pyromellitic dianhydride (PMDA) and oxydianiline (ODA). Raman spectroscopy was used to characterise the effects of non-stoichiometric deposition rates and substrate temperature on the chemical properties of the resulting PI film. Low fluxes and excess PMDA yield PI formation. High fluxes and excess PMDA thus ruling out the possibility of a one step process for PI formation. Defects that develop during processing of the polymer polyimide can adversely alter the dielectric properties and adhesion of polyimide thin films which are widely used, for semiconductors. Polyimide films can be cast or spin coated from solution or formed by direct vapor deposition.

Open PDF

Document Details

Document Type
Technical Report
Publication Date
May 15, 1991
Accession Number
ADA237467

Entities

People

  • C. M. Carlin
  • R. G. Pethe
  • W. N. Unertl

Organizations

  • University of Maine

Tags

Communities of Interest

  • Advanced Electronics
  • Materials and Manufacturing Processes
  • Weapons Technologies

DTIC Thesaurus Topics

  • Acquisition
  • Base Pressure
  • Chemistry
  • Civil Engineering
  • Dielectric Properties
  • Engineering
  • Films
  • High Vacuum
  • Military Research
  • Raman Spectra
  • Raman Spectroscopy
  • Reaction Mechanisms
  • Spectra
  • Spectroscopy
  • Thermal Stability
  • Universities
  • Vapor Deposition

Fields of Study

  • Materials science

Readers

  • Nanofabrication and Microfabrication.
  • Polymer Science and Engineering.
  • Thin Film Deposition Science.

Technology Areas

  • Microelectronics
  • Microelectronics - Graphene