Comparative Evaluation of Ultrafiltration/Microfiltration Membranes for Removal of Nitrocellulose (NC) Fines from Wastewater

Abstract

Nitrocellulose (NC) is a basic constituent for military gun propellants. NC wastewater is a byproduct of the NC manufacturing process. Crossflow microfiltration/ultrafiltration (MF/UF) may recover NC fines and allow the wastewater to be recycled. This bench-scale crossflow membrane filtration system was constructed to test the application of MF/UF technology to NC wastewater. This study was conducted in two phases. The results of Phase I were used to select a candidate membrane. In Phase II, a pilot-scale crossflow membrane filtration system was constructed to: (1) investigate the concentration polarization and fouling mechanism caused by NC fines during crossflow filtration of NC wastewater, (2) explore flux decline behavior of NC wastewater streams with various membranes, and (3) study the effects of operating parameters on flux decline behavior. This study found that: 1. UF membranes have a lower flux decline rate and a higher flux recovery than MF membranes, but UF membranes have a relatively low permeate production rate compared to MF membranes. 2. A critical membrane pore size of about 0.1 micron exists, at which point the worst flux performance occurs. 3. The cellulose-based hydrophilic membranes have the best flux performance.

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Document Details

Document Type
Technical Report
Publication Date
Jul 01, 1997
Accession Number
ADA332826

Entities

People

  • Byung-joon Kim
  • Mark M. Clark
  • Yonghun Lee

Organizations

  • Construction Engineering Research Laboratory

Tags

Communities of Interest

  • Biomedical
  • C4I
  • Weapons Technologies

DTIC Thesaurus Topics

  • Autoignition
  • Boundary Layer
  • Chemical Reaction Properties
  • Chemical Synthesis
  • Chemistry
  • Filtration
  • Hydrophilic Properties
  • Hydrophobic Properties
  • Manufacturing
  • Materials Laboratories
  • Materials Science
  • Measurement
  • Mixing
  • Mixtures
  • Particle Size
  • Stratified Fluids
  • Ultrafiltration

Fields of Study

  • Environmental science

Readers

  • Environmental Engineering
  • Manufacturing Engineering.
  • Rocket Propulsion.